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Beilstein J. Org. Chem. 2013, 9, 332–341, doi:10.3762/bjoc.9.38
Graphical Abstract
Figure 1: Structure of some O-linked glycans found on the cell surface of P. aeruginosa.
Scheme 1: Retrosynthetic analysis of D- and L-fucosamine building blocks.
Scheme 2: (A) Synthesis of aldehydes 6a and 6b. (B) Alkyne reduction by hydrosilylation–protodesilylation seq...
Scheme 3: Synthesis of D-fucosamine building blocks 8a and 8b.
Scheme 4: Epimerization of aldehyde 6a.
Scheme 5: Synthesis of L-fucosamine building block L-8a from D-Garner aldehyde.
Scheme 6: Synthesis of D- and L-fucosamine-containing mono- and disaccharides carrying the pentanolamine link...